Synthesis of a polymeric-based stationary phase for carbohydrate separation by high-pH anion-exchange chromatography with pulsed amperometric detection
β Scribed by Claudio Corradini; Danilo Corradini; Christian G. Huber; Gunther K. Bonn
- Publisher
- Elsevier Science
- Year
- 1994
- Tongue
- English
- Weight
- 925 KB
- Volume
- 685
- Category
- Article
- ISSN
- 1873-3778
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## Abstract A monodisperse polymerβbased anion exchanger was synthesized through a twoβstep swelling and polymerization method for the analysis of unmodified carbohydrates by reducedβdiameter column liquid chromatography with a pulsed amperometric detector. Separation characteristics were studied f
We have evaluated the high-pH anion-exchange chromatography with pulsed amperometric detection (HPAE-PAD) with respect to its suitability to establish a carbohydrate mapping database that would enable carbohydrate structural analysis by mere comparison of retention times. The suitability of HPAE-PAD