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Synthesis of a P-1-tethered photoaffinity label for inositol hexakisphosphate binding proteins

✍ Scribed by Jian Chen; Glenn D. Prestwich

Publisher: John Wiley and Sons
Year: 1996
Tongue: French
Weight: 354 KB
Volume: 38
Category: Article
ISSN: 0022-2135
DOI: 10.1002/(sici)1099-1344(199612)38:12<1113::aid-jlcr925>3.0.co;2-6

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✦ Synopsis

A new photoaffinity analog of inositol hexakisphosphate (InsPs, or phytic acid) was prepared for investigation of InsP6-binding proteins. The racemic P-l-(O-8aminohexyl) derivative of lnsP6 was synthesized in six steps from inositol, and a tritium-labeled benzophenone-containing photophore was attached in the final step to give P-1 [3H]BZDC-lnsP6 (sp. act. 35 Cilmmol).

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