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Synthesis of 5-Hydroxyalkylpyrimidines from Lactones 1,2

✍ Scribed by Fissekis, John D.; Myles, Arthur; Brown, George Bosworth

Book ID
120584733
Publisher
American Chemical Society
Year
1964
Tongue
English
Weight
501 KB
Volume
29
Category
Article
ISSN
0022-3263

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✍ Diane R. Wolk; Andrea Vasella; Fritz Schweikart; Martin G. Peter πŸ“‚ Article πŸ“… 1992 πŸ› John Wiley and Sons 🌐 German βš– 707 KB

The carbohydrate-derived lactone phenylsemicarbazones 3 and 4 were prepared from 5 and 8 (Scheme). Treatment with 4-phenylsemicarbazide gave 6 and 7 (77:23) and 9 and 10 (76:24), respectively. Oxidation of 6 and 9 by Cr0,-pyridine to 11 and 13, followed by deprotection, yielded 3 and 4. The structur