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Synthesis of 5- and 6-Hydroxymethylfluorescein Phosphoramidites

✍ Scribed by Adamczyk, Maciej; Chan, Clifford M.; Fino, James R.; Mattingly, Phillip G.

Book ID: 120064459
Publisher: American Chemical Society
Year: 2000
Tongue: English
Weight: 177 KB
Volume: 65
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo991449h

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The d-allo-and l-talo-hept-6-ynofuranosyluracil-derived phosphoramidites 11A and 11T were prepared in 9 ± 10% yield over eight steps from the previously described propargylic alcohols 1A and 1T, respectively. The corresponding nucleotides were incorporated into rU 14 by standard solid-phase synthesi