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Synthesis of 3-methyl-16-iodo-[carboxyl-14C] hexadecanoic acid (MIHA)

✍ Scribed by H. Ozem; C. Béney; C. Luu-Duc

Publisher: John Wiley and Sons
Year: 1996
Tongue: French
Weight: 270 KB
Volume: 38
Category: Article
ISSN: 0022-2135
DOI: 10.1002/(sici)1099-1344(199606)38:6<541::aid-jlcr869>3.0.co;2-e

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✦ Synopsis

Carbon-14 labelled fl-methyl-iodohexadecanoic acid (MIHA) was obtained in a four step sequence using Na14CN, starting from 15-tetrahydropyranyloxy-2-methyl-pentademol-p-toluene sulfonate z. The specific radioactivity was 55 mCi/mmol and the radiochemical yield 41% of the theoretical maximum.

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