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Synthesis of 3-amino and 3-alkylamino derivatives of isofervenuline. First instance of direct amination of the 1,2,4-triazine ring at position 3

✍ Scribed by A. F. Pozharskii; A. V. Gulevskaya; V. V. Kuz'menko

Book ID: 104785572
Publisher: Springer US
Year: 1988
Tongue: English
Weight: 149 KB
Volume: 24
Category: Article
ISSN: 0009-3122
DOI: 10.1007/bf00486689

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## Abstract A mixture of both geometrical isomers of hydrazones **3a‐3e** was obtained by the coupling reactions of pyrazole‐3‐diazonium salts __2a‐2d__ and benzenediazonium chloride **2e** with 2‐pyridylacetonitrile **1**. Hydrazones **3a‐3d** were cyclized to the corresponding 4‐amino‐3‐(2‐pyridy