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Synthesis of [26-2H3]brassinosteroids

✍ Scribed by Vladimir A Khripach; Vladimir N Zhabinskii; Olga V Konstantinova; Andrey P Antonchick; Bernd Schneider

Book ID: 117213477
Publisher: Elsevier Science
Year: 2002
Tongue: English
Weight: 150 KB
Volume: 67
Category: Article
ISSN: 0039-128X
DOI: 10.1016/s0039-128x(02)00004-1

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## Abstract The synthesis of 25‐hydroxycholecaleiferol‐(26, 27‐^3^H) is described. 25‐Oxo‐27‐norcholesta‐5, dien‐3β‐yl acetate is converted photochemically to 25‐oxo‐27‐norcholecalciferol‐3‐acetate, which is then reacted with tritiated methylmagnesium iodide and subsequently saponified to give 25‐h