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Synthesis of 2,4-diamino-6-piperidinylpvrimidine-3-oxide-3′,4′,;5′-3h(n) tritiated minoxidil

✍ Scribed by Terry J. Gilbertson

Publisher
John Wiley and Sons
Year
1976
Tongue
French
Weight
154 KB
Volume
12
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

Minoxidil‐3′,4′,;5′‐^3^H(N), 25.6 Ci/mM. has been synthesized by the reaction of piperidine‐3,4,5‐^3^H(N) with 2,4‐diamino‐6‐chloro‐pyrimidine‐3‐oxide. Purification was by paper chromatography. Minoxidil prepared in this way was shown to be suitable for radioimmunoassay and was stable for six months stored in MeOH at 4° C.

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