Synthesis of 2′,3′-dideoxy-2′,3′-α-methanocytidine
✍ Scribed by Andrew R. Beard; Paul I. Butler; John Mann; Neil K. Partlett
- Book ID
- 107725930
- Publisher
- Elsevier Science
- Year
- 1990
- Tongue
- English
- Weight
- 342 KB
- Volume
- 205
- Category
- Article
- ISSN
- 0008-6215
No coin nor oath required. For personal study only.
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5 0 -O-Benzoyl-2,3 0 -anhydrothymidine. 60% Methanol in water, retention time 13.1 min. \* 2 0 ,3 0 -Dideoxy-2 0 ,3 0 -didehydrothymidine. Solvents: A -water; B -methanol. Program: 0-40% B/A in 40 min, retention time 33.9 min. TLC was carried out on Silufol plates (Czech Republic). \* 5 0 -O-Benzo