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Synthesis of 2-substituted 1-benzyl-2,3,4,5-tetrahydro-1-benzazepines by palladium catalysis. Observation of a competitive β-hydride elimination pathway

✍ Scribed by Maryiam Qadir; Rachael E. Priestley; Thomas W.D.F. Rising; Thomas Gelbrich; Simon J. Coles; Michael B. Hursthouse; Peter W. Sheldrake; Neil Whittall; K.K.(Mimi) Hii

Publisher: Elsevier Science
Year: 2003
Tongue: French
Weight: 111 KB
Volume: 44
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(03)00676-2

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## Abstract An efficient, diastereoselective synthesis of substituted and unsubstituted 2,3,4,5‐tetrahydro‐1__H__‐1‐benzazepine‐5‐carboxylic esters has been developed based on the tandem reduction‐reductive amination reac tion. Catalytic hydrogenation of a series of 2‐(2‐nitrophenyl)‐5‐oxoalkanoic