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Synthesis of 2-Substituted 1-Benzyl-2,3,4,5-tetrahydro-1-benzazepines by Palladium Catalysis. Observation of a Competitive β-Hydride Elimination Pathway.

✍ Scribed by Maryiam Qadir; Rachael E. Priestley; Thomas W. D. F. Rising; Thomas Gelbrich; Simon J. Coles; Michael B. Hursthouse; Peter W. Sheldrake; Neil Whittall; K. K. Hii

Publisher: John Wiley and Sons
Year: 2003
Weight: 125 KB
Volume: 34
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200331186

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## Abstract An efficient, diastereoselective synthesis of substituted and unsubstituted 2,3,4,5‐tetrahydro‐1__H__‐1‐benzazepine‐5‐carboxylic esters has been developed based on the tandem reduction‐reductive amination reac tion. Catalytic hydrogenation of a series of 2‐(2‐nitrophenyl)‐5‐oxoalkanoic