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Synthesis of [2-(dimethylphosphino)ethyl]bis(trifluoromethyl)phosphine, (CH3)2PCH2CH2P(CF3)2

✍ Scribed by Leslie D. Field; Matthew P. Wilkinson

Book ID: 104256835
Publisher: Elsevier Science
Year: 1997
Tongue: French
Weight: 209 KB
Volume: 38
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(97)00469-3

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✦ Synopsis

The ethylene-bridged bisphosphine, [2-(dimethylphosphino)ethyllbis(trifluoromethyl)phosphine, [(CH~),PCH,CH,P(CF3)2], was synthesised in four steps from the unsymmetrical bisphosphine (CH0,PCH2CH2PH v using a new trifluoromethylation procedure employing CF3Br and hexaethylphosphorus triamide.

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