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Synthesis of 2-Arylbenzoxazoles from Flash Vacuum Pyrolysis of 2-Methoxy-N-(arenylidene)anilines

โœ Scribed by Chin-Hsing Chou; Yu-Tan Hsueh; Bo-Chi Wang

Book ID
112120383
Publisher
Chinese Electronic Periodical Services
Year
2011
Tongue
English
Weight
839 KB
Volume
58
Category
Article
ISSN
0009-4536

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Synthesis of pyridothietone by flash vac
Synthesis of pyridothietone by flash vacuum pyrolysis of 2-mercaptonicotinic acid
โœ Chin-Hsing Chou; Shao-Jung Chiu; Wei-Min Liu ๐Ÿ“‚ Article ๐Ÿ“… 2002 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 87 KB

The temperature dependence of products formed from flash vacuum pyrolysis (FVP) of 2-mercaptonicotinic acid 4 has been studied. FVP of 4 at 550ยฐC and ca. 1ร—10 -2 torr gave pyridothietone 3b and a trimer 5 as the major products. At higher temperature (800ยฐC), FVP of 4 gave 2-mercaptopyridine 6 as the