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SYNTHESIS OF 2-AMINO-1-PHENYL-1-PROPANOL AND ITS METHYLATED DERIVATIVES

✍ Scribed by HOOVER, FRED W.; HASS, HENRY B.


Book ID
111975520
Publisher
American Chemical Society
Year
1947
Tongue
English
Weight
320 KB
Volume
12
Category
Article
ISSN
0022-3263

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Synthesis of 1-[15N]amino-2-propanol hyd
✍ Katsumi Iida; Kuniaki Ohtaka; Masahiro Kajiwara πŸ“‚ Article πŸ“… 2007 πŸ› John Wiley and Sons 🌐 French βš– 92 KB

## Abstract 1‐[^15^N]Amino‐2‐propanol hydrochloride (**2**) was synthesized in three steps, i.e. Gabriel condensation of potassium [^15^N]phthalimide (**3**) with chloroacetone (**4**), reduction of the product ([^15^N]phthalimidoacetone (**5**)) with sodium borohydride, and hydrolysis in 33% total