โ Scribed by Timothy W. Hepburn; Gordon Lowe
No coin nor oath required. For personal study only.
A new synthesis of [^18^O]thionyl chloride has been developed which, for the first time, allows the product to be isolated in pure form.
๐ SIMILAR VOLUMES
In tho usual type of Scliifl's nitroiUetcr tlic measuring tubc ip of uniform borc nnd is graduntcd froin O to 100 C.C. in 1/5tli of a C.C. Tlic graduntioiis a t tlic lowcr end .of tlic scale arc practically useless, as in ordcr to frtc tlic nitrogen from tlic carbon dioxide used to drive it over, i
180]-Chlorocarbonylsulfenyl chloride with an isotopic purity of 92% was prepared in three steps starting with the [180]-hydrolysis of 2-ethyl-l,3-dioxolane to [' 80]-propanal, which was then converted to [180]-g-1 -methylpropyl ?-methyl dithiocarbonate, which was then chlorinated to give the title c
## Abstract Hydrazones **__12aโc__** and ketazines **__13aโc__** were prepared by the reaction of ketones **__11aโc__** with hydrazine hydrate depending on the temperature and the reaction time. Some ketone (aryl)hydrazone derivatives **__14a,c,e__** reacted with thionyl chloride to afford the chlo