𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Synthesis of 16α-3H androgen and estrogen substrates for 16α-hydroxylase

✍ Scribed by R. Cantineau; P. Kremers; J. De Graeve; A. Cornelis; P. Laszlo; J.E. Gielen; R. Lambotte

Book ID
119481462
Publisher
Elsevier Science
Year
1981
Tongue
English
Weight
632 KB
Volume
37
Category
Article
ISSN
0039-128X

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Synthesis of [16,16,17α-2H3] estradiol a
Synthesis of [16,16,17α-2H3] estradiol and [14α,15,15–2H3] estrone of high isotopic purity
✍ Ian J. Massey; Laszlo Tökés 📂 Article 📅 1981 🏛 John Wiley and Sons 🌐 French ⚖ 410 KB

## Abstract The title compounds, each of high isotopic purity, were synthesized as internal standards for the mass spectral quantitation of estradiol and estrone. The [^2^H~3~] estradiol **3** was obtained from estrone (**1**) by alkaline H/^2^H exchange of the C‐16 protons and LiAl^2^LH~4~ reducti

A simple and efficient synthesis of [3α-
A simple and efficient synthesis of [3α-3H]5α-androst-16-en-3β-ol
✍ S. Ren; D. Hesk; P. McNamara; D. Koharski 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 French ⚖ 110 KB

## Abstract An efficient one step synthesis of [3__α__‐^3^H]5__α__‐androst‐16‐en‐3__β__‐ol by NaBT~4~ reduction of a ketone precursor is described. The specific activity of the product was 21.6 Ci/mmol with a radiochemical purity >99%. Synthesis of the precursor, 5__α__‐androst‐16‐en‐3‐one, from co