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Synthesis of [16]annulene 1,4:7,10-dioxide and the verification of an induced paramagnetic ring current

✍ Scribed by Haru Ogawa; Masaharu Kubo; Iwao Tabushi


Publisher
Elsevier Science
Year
1973
Tongue
French
Weight
242 KB
Volume
14
Category
Article
ISSN
0040-4039

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The synthesis and characterization of the two macrocyclic s&ides, 1,4,7,lO,l3,16,19-heptathiaheneicosane (21-S-7) and 1,4,7,10,13,16,19,22-octathiatetraeicosane (24-S-8), are describedstarting from different combmationsof dithiols and dichlorides of differing chain lengths. C&O, is used for the cycl