## Abstract ^14^C‐Labelled __N__‐(2‐chloro‐3,4‐dimethoxybenzylideneamino)guanidinium acetate has been synthesized as a part of a four‐step procedure which involved decarboxylation of 2‐chloro‐3,4‐dimethoxybenzoic acid by Pb(OAc)~4~ to give 2‐chloro‐3,4‐dimethoxy‐1‐iodobenzene, followed by a selecti
Synthesis of 14C-labelled 2-(p-chloro-α-hydroxybenzyl)-benzimidazole (HBBPC)
✍ Scribed by A. Durand; C. Beney; C. Luu Duc; Cl. Agnius Delord
- Publisher
- John Wiley and Sons
- Year
- 1981
- Tongue
- French
- Weight
- 118 KB
- Volume
- 18
- Category
- Article
- ISSN
- 0022-2135
No coin nor oath required. For personal study only.
✦ Synopsis
Abstract
p‐Chloro[^14^C]mandelic acid 2 was prepared from [^14^C]potassium cyanide and p‐chlorobenzaldehyde 1. The condensation of p‐chloro[^14^c] mandelic acid with 1,2‐diamino benzene 3 gave the title benzimidazole 4 labelled at the carbon atome 2 of the heterocyclic ring.
📜 SIMILAR VOLUMES
## Abstract Erythro‐ and threo‐ isomers of α‐(2‐piperidyl)‐2,8‐bis‐(triflucoromethyl)‐4‐quinolinemethanol‐α‐^14^C hydrochloride and methanesulfonate were prepared from labeled carbon dioxide for metabolic and pharmacological studies. Intermediates were 2,8‐bis(trifluoromethyl) cinchoninic‐carboxy‐^
## Abstract The preparation of ^14^C‐labelled 11β, 21‐dihydroxy‐3,20‐dioxy‐pregna‐1,4‐dieno[ 17α, 16α‐d]‐2′‐methyloxazoline‐21‐acetate and of 9α‐fluoro‐11β,21‐dihydroxy‐3,20‐dioxopregna‐l,4‐dieno[ 17α,16α ]‐2′‐methyloxazoline‐21‐acetatelNote that [17α., 160α‐d] does not refer to deuterium labelling
## Abstract Synthetic procedures for N‐(2‐p–azidophenylethyl)‐norlevorphanol (9) labeled with ^14^C and ^3^H at the 1‐position of the 2‐phenylethyl moiety are presented. A process for synthesis of p‐nitrophenylacetic‐1‐^14^C acid from p‐chloro‐nitrobenzene and methyl cyano‐^14^C‐acetate is describe