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Synthesis of 1,3,4-trifluoroisoquinoline by copyrolysis of 2,3,5,6-tetrafluoropyridine-4-sulfonyl chloride with butadiene

✍ Scribed by V. G. Kolechkina; A. M. Maksimov; V. E. Platonov; O. I. Osina

Book ID
110275361
Publisher
Springer
Year
2001
Tongue
English
Weight
229 KB
Volume
50
Category
Article
ISSN
1573-9171

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## Abstract A concise method for the synthesis of the title compounds has been developed, which involves condensation of lactols with methylthiomethyl p‐tolyl sulfone, followed by mesylation and further cyclisation of the elimination products by refluxing with excess of sodium iodide in dimethyl fo