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Synthesis of 1,3-dioxolanes from acetylenic 1,2,5-triols

✍ Scribed by Sh. M. Musantaeva; K. O. Akimova; A. V. Shchelkunov

Publisher
Springer US
Year
1988
Tongue
English
Weight
170 KB
Volume
24
Category
Article
ISSN
0009-3122

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## Abstract The acid catalyzed reaction of glycerol‐d~5~ with bromoacetaldehyde dimethyl acetal affords the corresponding 2‐bromomethyl‐4‐hydroxymethyl‐1,3‐dioxolane, which was treated with lithium iodide in 2‐butanone to afford the pentadeuterated domiodol 1 in high isotopic purity.