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Synthesis of 10-(4-methyl-1-piperazinyl)thieno[3,2-b][1,5]benzoxazepines

✍ Scribed by Carlos Corral; Jaime Lissavetzky; Ana M. Valdeolmillos

Book ID: 112128001
Publisher: Journal of Heterocyclic Chemistry
Year: 1985
Tongue: English
Weight: 183 KB
Volume: 22
Category: Article
ISSN: 0022-152X
DOI: 10.1002/jhet.5570220542

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## Abstract A new series of 4‐(4‐methylpiperazin‐1‐yl)thieno[2,3‐__b__][1,5]benzoxazepines **1a‐k** has been synthesized from 4‐bromo‐2‐methylthiophene **6** or ethyl 2‐amino‐4,5‐dimethyl‐3‐thiophencarboxylate **10**. Preparation of the key intermediate thieno[2,3‐__b__][1,5]benzoxazepine‐4(5__H__)