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Synthesis of 1-methyl-3H-1,4-benzodiazepline-2,5 (1H,4H) -dione and derivatives

โœ Scribed by Cheuk-Man Lee

Book ID
112121247
Publisher
Journal of Heterocyclic Chemistry
Year
1964
Tongue
English
Weight
282 KB
Volume
1
Category
Article
ISSN
0022-152X

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## Abstract Pentadeuteriophenyl clobazam 5 was synthesized in essentially quantitative isotopic purity, and characterized by ^1^Hโ€NMR and mass spectroscopy. The title compound was found to be โ‰ฅ98% pure by HPLC, and its retention time (t~R~ 6.17 min) was less than that of an authentic clobazam stand