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Synthesis of 1-(aminooxy)-4-[(3-nitro-2-pyridyl)dithio]butane and 1-(aminooxy)-4-[(3-nitro-2-pyridyl)dithio]-2-butene, novel heterobifunctional crosslinking reagents

โœ Scribed by Webb, Robert R.; Kaneko, Takushi


Book ID
127238706
Publisher
American Chemical Society
Year
1990
Tongue
English
Weight
551 KB
Volume
1
Category
Article
ISSN
1043-1802

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โœ Vijendra Kumar Fulwa; Rojalin Sahu; Himanshu Sekhar Jena; Vadivelu Manivannan ๐Ÿ“‚ Article ๐Ÿ“… 2009 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 397 KB

a b s t r a c t Heating a neat 1:2 mixture of 2-picolylamine and 2-cyanopyridine followed by treatment of the resultant red gummy substance with aqueous KOH resulted in the isolation of 2,4,5-tris(2-pyridyl)imidazole (1a) as the major product and N-(3-(2-pyridyl)imidazo[1,5-a]pyridine)picolinamidine