The structures of the title compounds C 26 H 37 N 2 O 2 Sn (I) and C 14 H 9 IN 2 O 2 (II) were determined by singlecrystal X-ray diffraction technique. Compound I crystallizes in the triclinic space group P1 with a = 9.560(3) ร , b = 16.899(6) ร , c = 17.872(5) ร , ฮฑ = 65.957(7)ยฐ, ฮฒ = 83.603(5)ยฐ, ฮณ๏จ =
โฆ LIBER โฆ
Synthesis of 1-(3-trideuteromethoxy-4-hydroxyphenyl)-[1,2,2-2H3]-ethyleneglycol ([2H6]MHPG)
โ Scribed by S Murray; T A Baillie; D S Davies
- Publisher
- John Wiley and Sons
- Year
- 1981
- Tongue
- French
- Weight
- 197 KB
- Volume
- 18
- Category
- Article
- ISSN
- 0022-2135
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โฆ Synopsis
Abstract
The four stage synthesis of a hexadeuterated analogue of the noradrenaline metabolite 3โmethoxyโ4โhydroxyphenylethylene glycol (MHPG) is described. The overall yield from 3โtrideuteromethoxyโ4โhydroxyacetophenone is 29%.
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## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract, please click on HTML or PDF.
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