Synthesis, nuclear magnetic resonance, and X-ray structural investigations of 1,6-diaza-9,12-dioxacyclotetradeca-2,5-dione
✍ Scribed by P. Gluziński; J. W. Krajewski; S. Kasprzyk; P. Sałański; T. Stankiewicz; J. Jurczak
- Publisher
- Springer
- Year
- 1992
- Tongue
- English
- Weight
- 309 KB
- Volume
- 22
- Category
- Article
- ISSN
- 1572-8854
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## Abstract The molecular structures of the title compounds 3 and 5 were investigated by NMR and X‐ray structural methods. The NMR results suggest two equivalent halves for both molecules. The X‐ray study shows an approximate mirror plane for 3 and an approximate twofold axis for a significant port
## Qystals of NiL(NCS)2 (L = 2,3:11,12-dibenzo-1,13dioxa-5,9diaza-2,11-cyclopentadecadiene), obtained by adding the ligand in buthanol to a methanolic solution of KSCN and Ni(ClO.&.HzO, are triclinic (PI), with cell dimensions: a = 9.836(2), b = 18.825(7), c = 8.003(4) A, (Y = 81.57(5), fl = 64.99
## Abstract For Abstract see ChemInform Abstract in Full Text.