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Synthesis, NMR analysis and X-ray crystal structure of 6,12-bis(4-fluorophenyl)-3,9-dioxatetraasterane

✍ Scribed by Xiu-Qing Song; Hui-Qin Wang; Hong Yan; Cheng-Liang Ni; Ru-Gang Zhong

Book ID: 113806143
Publisher: Elsevier Science
Year: 2011
Tongue: English
Weight: 659 KB
Volume: 1006
Category: Article
ISSN: 0022-2860
DOI: 10.1016/j.molstruc.2011.09.056

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## Abstract magnified image A series of chiral, nonracemic oxadiazines have been prepared from (1__R__,2__S__)‐ephedrine, (1__R__,2__S__)‐norephedrine, and L‐phenylalaninol. The synthesis of the __Ephedra__‐based oxadiazines was accomplished by a process of __N__‐nitrosation, reduction, acylation,