✦ LIBER ✦

Synthesis, isolation and immunochemical characterization of N-(carboxymethyl-3H)-D-lysergamide

✍ Scribed by Jeffrey L. Winkelhake; Edward W. Voss Jr.

Publisher: John Wiley and Sons
Year: 1974
Tongue: French
Weight: 416 KB
Volume: 10
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2590100315

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

Covalent amide linkage of glycine‐2‐^3^H to the non‐hallucinogenic derivative, d‐lysergic acid (LSA), by carbodiimide activation results in a lysergic acid analogue which has potential use in biochemical studies of the mode of action, metabolism and immunology of d‐lysergic acid diethylamide (LSD). Optimal conditions for the reaction and isolation of the product, N‐(carboxymethyl‐^3^H)‐d‐lysergamide, were determined. The product was analyzed by radioimmune assay and by equilibrium dialysis with highly specific antibody to the lysergyl moiety.

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