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ChemInform Abstract: Synthesis, Characterization, and Explosive Properties of the Nitrogen-Rich Borazine [H3N3B3(N3)3].

✍ Scribed by Robert T. Paine; Wolfgang Koestle; Theodore T. Borek; Gary L. Wood; Eugene A. Pruss; Eileen N. Duesler; Michael A. Hiskey

Publisher: John Wiley and Sons
Year: 2010
Weight: 34 KB
Volume: 30
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199943022

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✦ Synopsis

Synthesis, Characterization, and Explosive Properties of the

-The known 2,4,6triazidoborazine (III) is synthesized in an improved way. Single crystal XRD analysis confirms its triclinic structure (space group P1, Z = 4). The azidopentamethylborazine (VII) is synthesized and characterized for the first time. The Staudinger reactivity of the azides with PPh 3 is studied and (III) is found to produce (V), which crystallizes in the orthorhombic space group P2 1 2 1 2 1 with Z = 4. -(PAINE,

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