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Synthesis, isolation and characterisation of β-sitosterol and β-sitosterol oxide derivatives

✍ Scribed by McCarthy, Florence O.; Chopra, Jay; Ford, Alan; Hogan, Sean A.; Kerry, Joe P.; O'Brien, Nora M.; Ryan, Eileen; Maguire, Anita R.


Book ID
120382912
Publisher
Royal Society of Chemistry
Year
2005
Tongue
English
Weight
174 KB
Volume
3
Category
Article
ISSN
1477-0520

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Synthesis of β-sitosterol-3-14C
✍ P. P. H. H. L. Otto; A. C. Besemer; W. H. J. M. Wientjens 📂 Article 📅 1970 🏛 John Wiley and Sons 🌐 French ⚖ 581 KB

## Abstract The synthesis of β‐sitosterol‐3‐^14^C, specific activity 5 mCi/mM, radiochemical purity ≥98 %, is described. Starting from stigmasterol, the complete synthesis consists of eleven reaction steps. It is based on methods described in the literature. For some of the steps, a considerable im