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Gram-scale chromatographic purification of β-sitosterol: Synthesis and characterization of β-sitosterol oxides

✍ Scribed by Xin Zhang; Philippe Geoffroy; Michel Miesch; Diane Julien-David; Francis Raul; Dalal Aoudé-Werner; Eric Marchioni

Book ID
116891848
Publisher
Elsevier Science
Year
2005
Tongue
English
Weight
313 KB
Volume
70
Category
Article
ISSN
0039-128X

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Synthesis of β-sitosterol-3-14C
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✍ P. P. H. H. L. Otto; A. C. Besemer; W. H. J. M. Wientjens 📂 Article 📅 1970 🏛 John Wiley and Sons 🌐 French ⚖ 581 KB

## Abstract The synthesis of β‐sitosterol‐3‐^14^C, specific activity 5 mCi/mM, radiochemical purity ≥98 %, is described. Starting from stigmasterol, the complete synthesis consists of eleven reaction steps. It is based on methods described in the literature. For some of the steps, a considerable im