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Synthesis, Crystal Structure and Luminescence Property of a Chiral Magnesium (II) Mixed-ligand Complex [Mg(H2O)2(phen)(HBDC)2](phen)

โœ Scribed by Ai-xiang Chen; Gang Liu; Hui Li; Ji-de Wang; Fan Yue

Publisher
Springer
Year
2010
Tongue
English
Weight
604 KB
Volume
41
Category
Article
ISSN
1572-8854

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Dark blue plate-like crystals of [Cu 2 (phen) 2 (H 2 O) 2 (OH) 2 ](HCO 3 ) 2 ยด6 H 2 O were obtained from a CH 3 OHยฑH 2 O solution containing CuCl 2 , 1,10-phenanthroline (phen), sebacic acid and Na 2 CO 3 . The crystal structure (triclinic, P 1 (no. 2), a = 8.118(1), b = 9.624(1), c = 10.536(1) A รŠ

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Blue crystals of Cu 2 (phen) 2 (H 2 O) 2 (C 5 H 6 O 4 ) 2 were obtained from a CH 3 OHยฑH 2 O solution containing CuCl 2 , 1,10-phenanthroline (phen), glutaric acid and Na 2 CO 3 . The crystal structure (monoclinic, P2 1 /c (no. 14), a = 10.271(1), b = 10.595(1), c = 15.585(1) A รŠ , b = 107.105(3)ยฐ,