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Synthesis, Conformational Polymorphism, and Construction of a G − T Diagram of 2-[(2-Nitrophenyl)amino]-3-thiophenecarbonitrile

✍ Scribed by Li, Hui; Stowell, Joseph G.; Borchardt, Thomas B.; Byrn, Stephen R.

Book ID
117988356
Publisher
American Chemical Society
Year
2006
Tongue
English
Weight
413 KB
Volume
6
Category
Article
ISSN
1528-7483

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Solid-solid transformation of 5-methyl-2-[(4-methyl-2-nitrophenyl)amino]-3-thiophenecarbonitrile from the dark-red to the red form was investigated. By controlled crystallization, the dark-red form was prepared and the crystals were sieved into fractions: coarse (>250 mm), medium (125-177 mm), and f