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Conformational and color polymorphism of 5-methyl-2-[(2-nitrophenyl)amino]-3-thiophenecarbonitrile

✍ Scribed by G. A. Stephenson; T. B. Borchardt; S. R. Byrn; J. Bowyer; C. A. Bunnell; S. V. Snorek; L. Yu


Book ID
102917695
Publisher
John Wiley and Sons
Year
1995
Tongue
English
Weight
573 KB
Volume
84
Category
Article
ISSN
0022-3549

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Solid-solid transformation of 5-methyl-2-[(4-methyl-2-nitrophenyl)amino]-3-thiophenecarbonitrile from the dark-red to the red form was investigated. By controlled crystallization, the dark-red form was prepared and the crystals were sieved into fractions: coarse (>250 mm), medium (125-177 mm), and f