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Synthesis, characterization and diels-alder extension of cyclopentadiene telechelic polyisobutylene

โœ Scribed by J. P. Kennedy; G. M. Carlson; K. Riebel

Publisher
Springer
Year
1983
Tongue
English
Weight
395 KB
Volume
9
Category
Article
ISSN
0170-0839

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โœ Kennedy, J. P. ;Carlson, G. M. ๐Ÿ“‚ Article ๐Ÿ“… 1983 ๐Ÿ› John Wiley and Sons โš– 648 KB

## Abstract Telechelic polyisobutylenes with silylcyclopentadiene termini (CpSiโ€PIBโ€SiCp) were prepared, starting with ฮฑ,ฯ‰โ€di(__t__โ€chloro)polyisobutylene and followed by dehydrochlorination, hydrosilylation, and cyclopentadienylation. The prepolymer was characterized and found to have a terminal f

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Irradiation of 1-phenylphosphole oxide-cyclopentadiene adduct gave a caged product, whereas similar irradiation of 1,2,5-triphenylphosphole oxidecyclopentadiene adduct afforded a cleavaged product. Previous studies 2) from this laboratory showed that the Diels-Alder dimer of 1-phenylphosphole oxide