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Synthesis, characterization and crystal structures of three new inorganic dinuclear diperoxo complexes of W(VI) and Mo(VI); Rb2{O[WO(O2)2H2O]2}·H2O, Rb2{O[MoO(O2)2H2O]2}·H2O and Cs2{O[MoO(O2)2]2}

✍ Scribed by M. Grzywa; W. Nitek; W. Łasocha

Publisher
Elsevier Science
Year
2009
Tongue
English
Weight
590 KB
Volume
919
Category
Article
ISSN
0022-2860

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Synthesis, characterization and crystal
Synthesis, characterization and crystal structures of three dinuclear diperoxo complexes of Mo(VI): K2{O[MoO(O2)2H2O]2}·2H2O, (C6H8N,NH4){O[MoO(O2)2H2O]2} and (C6H8N,Na){O[MoO(O2)2H2O]2}
✍ M. Grzywa; W. Nitek; W. Łasocha 📂 Article 📅 2008 🏛 Elsevier Science 🌐 English ⚖ 526 KB

The crystal structures of three dinuclear diperoxo compounds have been determined from single-crystal X-ray diffraction data. All title compounds crystallize as yellow needle-shaped crystals in the triclinic space group P 1(2). ( 1 where 2-MepyH denotes 2-methylopyridine, crystallize with a = 6.733