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Synthesis, characterization and crystal structure of bis{2-methoxy-6-[(2-diethylaminoethylimino)methyl]phenolato}thiocyanatocobalt(III) perchlorate

✍ Scribed by San-Jun Peng; Zhong-Lu You

Publisher
Springer
Year
2007
Tongue
English
Weight
515 KB
Volume
37
Category
Article
ISSN
1572-8854

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In a facile carbon-acid condensation reaction of bis(2-aminomethylpyridine)copper(II) with nitroethane and formaldehyde in basic MeOH the N,N' -bis(2-pyridylmethylene)-l,3-diamino-2-methyl-2-nitropropane)copper~I~) cation is produced in essentially quantitative yield. The perchlorate salt crystalliz