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Synthesis and X-Ray Structures of New Macrocyclic Thioethers

✍ Scribed by Mlinarić-Majerski, Kata ;Pavlović, DražEn ;Luić, Marija ;Kojić-Prodić, Biserka

Publisher
Wiley (John Wiley & Sons)
Year
1994
Tongue
English
Weight
325 KB
Volume
127
Category
Article
ISSN
0009-2940

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✦ Synopsis

tetrathiacyclooctadecane (3) have been obtained by intermolecular cyclization of 1,3-bis(2-bromoethyl)adamantane (4)

with thioacetamide using a high-dilution technique. The reaction is concentration-dependent. The crystal structures of 1, 2, and 3 have been determined by single-crystal X-ray diffraction.

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The molecular basis of sweet taste was investigated by carrying out the crystal state conformational analysis by X-ray diffraction of the following dipeptide taste ligands: N-3,3-dimethylbutyl-aspartylphenylalanine methyl ester, I (N-DMB-Asp-Phe-OMe), its sodium salt (N-DMB-Asp-Phe-ONa), II, asparty