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Synthesis and X-ray crystal structure of tetraethylammonium bis[1,2-di(carbomethoxy)ethane-1,2-dithiolato]oxotechnetate(V)

✍ Scribed by Giuliano Bandoli; Marino Nicolini; Ulderico Mazzi; Hartmut Spies; Rudolf Munze

Publisher
Springer
Year
1984
Tongue
English
Weight
326 KB
Volume
9
Category
Article
ISSN
0340-4285

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✍ Harald MΓΌller; Anna Puig Molina; B. Zh. Narymbetov; L. V. Zorina; S. S. Khasanov πŸ“‚ Article πŸ“… 1998 πŸ› John Wiley and Sons 🌐 German βš– 112 KB πŸ‘ 1 views

The title compounds were prepared from 1,3,4,6tetrathiapentalene-2,5-dione (1) in one step via the in situ The X-ray single crystal structure of (Et 4 N) 2 [Zn(dmid) 2 ] (3 a) gave the tetragonal space group P4 3 2 1 2 with a = b = 13.810(2) A Ê , c = 16.480(3) A Ê , and Z = 4. (n-Bu 4 N) 2 [Zn(dmi