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Synthesis and thermal decomposition of a novel zirconium acetato-propionate cluster: [Zr12]

✍ Scribed by Sarah Petit; Stéphanie Morlens; Zeming Yu; Dominique Luneau; Guillaume Pilet; Jean-Louis Soubeyroux; Philippe Odier

Book ID: 113914152
Publisher: Elsevier Science
Year: 2011
Tongue: English
Weight: 341 KB
Volume: 13
Category: Article
ISSN: 1293-2558
DOI: 10.1016/j.solidstatesciences.2010.12.041

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The title compound is obtained from reactions of \(\mathrm{CsI}, \mathrm{ZrI}_{4}, \mathrm{Zr}\), and \(\mathrm{C}\) in sealed \(\mathrm{Ta}\) at \(800^{\circ} \mathrm{C}\) (but not at \(850^{\circ} \mathrm{C}\) ). Both \(\mathrm{Zr}_{6} \mathrm{I}_{12} \mathrm{C}\) and \(\mathrm{Zr}_{6} \mathrm{I}_