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Synthesis and Study of Janus Bis(carbene)s and Their Transition-Metal Complexes

✍ Scribed by Dimitri M. Khramov; Andrew J. Boydston; Christopher W. Bielawski


Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
127 KB
Volume
118
Category
Article
ISSN
0044-8249

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Atropisomerism of Transition Metal Carbe
✍ Prof. Dr. Henri Brunner; Prof. Dr. Ernst Otto Fischer; Dipl.-Chem. Manfred Lappu πŸ“‚ Article πŸ“… 1971 πŸ› John Wiley and Sons 🌐 English βš– 201 KB πŸ‘ 2 views

10 ml, and chromatographed on a silica gel column (Merck 0.05 to 0.2 mm; column dimensions 40 x 2 cm) at 0Β°C with hexane/benzene (4 : 1). The yellow zone is collected, the solvent removed in a high vacuum, and the residue recrystallized twice from n-pentane : pale yellow needles, m. p. 45 "C ; yield