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Synthesis and structures of two thermally stable sodides with the macrocyclic complexant hexamethyl hexacyclen

✍ Scribed by Kuchenmeister, Mark E.; Dye, James L.

Book ID
125977062
Publisher
American Chemical Society
Year
1989
Tongue
English
Weight
543 KB
Volume
111
Category
Article
ISSN
0002-7863

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First example of thermally stable hyperv
First example of thermally stable hypervalent bismuth ate complex (12-Bi-6) with two bidentate ligands: Synthesis and structure
✍ Kin-ya Akiba; Keisuke Ohdoi; Yohsuke Yamamoto πŸ“‚ Article πŸ“… 1989 πŸ› Elsevier Science 🌐 French βš– 272 KB

A remarkably stable hexacoordinate bismuth ate complex (12) with two bidentate ligands was synthesized by the reaction of a pentacoordinate bismuth compound bearing a Bi-Cl bond (7\_) with a dilithiated reagent (2\_). The complex was stable up to 150 OC and was decomposed by water to afford an alcoh