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Synthesis and Structures of Titanium and Zirconium Trisiloxides

✍ Scribed by Krempner, Clemens; Jäger-Fiedler, Ulrike; Köckerling, Martin; Reinke, Helmut

Book ID
120285838
Publisher
American Chemical Society
Year
2009
Tongue
English
Weight
246 KB
Volume
28
Category
Article
ISSN
0276-7333

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Metallacyclodisiladiazanes of Titanium a
Metallacyclodisiladiazanes of Titanium and zirconium; Synthesis, Structure and Polymerization Studies
✍ Jäger, Felix ;Roesky, Herbert W. ;Dora, Hendrik ;Shak, Syed ;Noltemeyer, Mathias 📂 Article 📅 1997 🏛 Wiley (John Wiley & Sons) 🌐 English ⚖ 541 KB

A series of metallacyclodisiladiazanes has been prepared. Lithiated (SiMe2NHtBu)z (1) reacts with TiC1, . 2 THF to give (SiMe2NtBu)2TiClz (4). Methylation or fluorination of 4 leads to (SiMe2NtBu)2TiMe, (8) and (SiMezNtBu)zTiFz (9), respectively. The reaction of ZrCL . 2 THF with lithiated 1 or [Si-