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Synthesis and structure proof of a vitamin D3 metabolite, 25(s),26-dihydroxycholecalciferol

✍ Scribed by Partridge, John J.; Shiuey, Shian Jan; Chadha, Naresh K.; Baggiolini, Enrico G.; Blount, John F.; Uskokovic, Milan R.

Book ID: 120437185
Publisher: American Chemical Society
Year: 1981
Tongue: English
Weight: 333 KB
Volume: 103
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja00395a061

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## Abstract The 1α, 25, 26‐trihydroxy metabolite of vitamin D~3~, isolated from bovine serum, was shown to possess the (25 __S__)‐configuration by HPLC. comparison of the 1, 3, 26‐triacetate derivative with authentic (25 __R__)‐ and (25 __S__)‐samples. The convergent synthesis of (25 __R__)‐1α, 25,