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Synthesis and structure of [Zn8(HPO4)8(H2PO4)8]•[(C2H8N)8]•4H2O

✍ Scribed by P. Reinert; N. Zabukovec Logar; J. Patarin; V. Kaucic

Publisher
Elsevier Science
Year
1998
Tongue
English
Weight
556 KB
Volume
35
Category
Article
ISSN
0992-4361

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✦ Synopsis

A chain-like zincophosphate [Zns(HPO4)8(H2PO4)8]*[(C2HsN)s] -4H20 was obtained at room temperature from a ZnO/PzOs/dimethylamine/H20 mixture. The crystal structure was determined by single crystal X-ray diffraction. The symmetry is monoclinic a=l,26450(7)nm, b=l.08477(5)nm, c=1.46311(4)nm, 13=98.793(5) °, space group Co. The structure consists of chains of zinc-corner-sharing Zn2P204 four rings. The negative charge of the chains is compensated by the protonated dimethylamine. The characterization by 31p solid state nmr spectroscopy is also reported.

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