Synthesis and Structure of ThTe2I2
β Scribed by Frank Rocker; Wolfgang Tremel
- Publisher
- John Wiley and Sons
- Year
- 2001
- Tongue
- German
- Weight
- 99 KB
- Volume
- 627
- Category
- Article
- ISSN
- 0372-7874
No coin nor oath required. For personal study only.
π SIMILAR VOLUMES
Figure 1. ORTEP drawing of 5 (50 % probability thermal ellipsoids for all non-hydrogen atoms, perchlorate anion is omitted for clarity). Selected bond lengths [Γ€] and angles [8]: S1-N1 1.526(2), S1-C1 1.695(2), S1-C2 1.780(3), S1-C3 1.802(3), S2-N2 1.531(2), S2-C1 1.691(2), S2-C4 1.788(3), S2-C5 1.8
Reaction of K[(SePPh 2 ) 2 N] with [Te(tu) 4 ]Cl 2 (tu β«Χ‘β¬ thiourea) in methanol gave [Te{(SePPh 2 ) 2 N} 2 ], (1), while reaction of K[(SPPh 2 ) 2 N] with 4-MeOPhTeCl 3 in methanol gave [4-MeOPhTe-{(SPPh 2 ) 2 N}] 2 , ( 2). The crystals of 1 are triclinic and contain centrosymmetric molecules. The