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Synthesis and Structure of Novel Double Flexible Spacer Bridged Biscalix[4]arenes

✍ Scribed by Xian-Shun Zeng; Lin-Hong Weng; Lang-Xing Chen; Hong-Fang Ju; Xue-Bing Leng; Xi-Wen He; Zheng-Zhi Zhang


Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
423 KB
Volume
19
Category
Article
ISSN
0256-7660

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Syntheses of nine novel phanes derived from 4,4Ј-bipyridine methyl)pyridine (1) to furnish compounds 16-18 in low yield. Temperature-dependent NMR-spectroscopic studies of the incorporating new spacer elements are described together with their structural and spectroscopic properties. Starting macro