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Synthesis and Structure of Hypervalent Antimony Compounds Bearing Antimony-Iron Bonds

✍ Scribed by Yamamoto, Yohsuke; Okazaki, Michiko; Wakisaka, Yukiya; Akiba, Kin-ya

Book ID
120974008
Publisher
American Chemical Society
Year
1995
Tongue
English
Weight
658 KB
Volume
14
Category
Article
ISSN
0276-7333

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A hypervalent arsorane with an As-Fe bond [6: Rf 2 As\*FeCp(CO) 2 (Rf: o-C 6 H 4 C(CF 3 ) 2 O-)] was synthesized by the reaction of the arsoranide anion (4-Et 4 N: Rf 2 As\* -Et 4 N ‫ם‬ ) with CpFe(CO) 2 I (5) in the presence of AgBF 4 . Diastereomeric arsoranes {7a and 7b: Rf 2 As\*Fe\*Cp(CO)(PPh 3