Synthesis and structure of Cu1+4Mo6+5O17
β Scribed by E.M. McCarron III; J.C. Calabrese
- Publisher
- Elsevier Science
- Year
- 1986
- Tongue
- English
- Weight
- 737 KB
- Volume
- 65
- Category
- Article
- ISSN
- 0022-4596
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NH 4 ) 2 [Mo 6 Cl 14 ] Β΄H2 O (1) was prepared from reactions of MoCl 2 in ethanol with aqueous NH 4 Cl solution. It crystallizes in the monoclinic space group I2/a (no. 15), Z = 4 with a = 912.3(1), b = 1491.2(2), c = 1724.8(2) pm, b = 92.25(1)Β°; R1 = 0.023 (based on F values) and wR2 = 0.059 (based