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Synthesis and Structure of a Triruthenium Complex Containing a Face-Capping Pyridine Ligand

โœ Scribed by Takashi Kawashima; Toshiro Takao; Hiroharu Suzuki

Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
123 KB
Volume
118
Category
Article
ISSN
0044-8249

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โœ Reisgys, Martina ;Spies, Hartmut ;Johannesn, Bernd ;Pietzsch, Hans-Jergen ;Leibn ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› Wiley (John Wiley & Sons) ๐ŸŒ English โš– 493 KB

Neutral oxorhenium(V) complexes with dithioether ligands of the general formula [ReOX3(RS[CHz]2SR)], X = C1, Br, R = nBu, Et, Bzl were synthesized. Ammonium perrhenate reacts in concentrated hydrochloric acid with dithiaalkanes (RS[CH2I2SR, R = nBu, Et, Bzl) dissolved in glacial acetic acid to give