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Synthesis and Structure of a (Diphosphoxane)rhodium(I) Complex. Novel Reaction with CO To Liberate a Phosphinidene Oxide

✍ Scribed by Wang, Kun; Emge, Thomas J.; Goldman, Alan S.

Book ID: 126919958
Publisher: American Chemical Society
Year: 1994
Tongue: English
Weight: 402 KB
Volume: 13
Category: Article
ISSN: 0276-7333
DOI: 10.1021/om00017a088

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## Abstract An exploration of the Cu(I)‐L system under hydrothermal conditions, has led to the isolation of a novel framework [Cu(I)(L)]~n~ (**1**) (L = bis(3,3‐dimethyl‐4,4‐dihydro‐1H‐pyrazol‐4‐yl)methane). Single‐crystal X‐ray analysis reveals that it crystallizes in the monoclinic, space group C